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"The abundance of graphite waste can be processed into valuable materials; one alternative is by making it into an adsorbent. Graphite-based adsorbent modification can be accomplished by adding magnetite nanoparticles Fe3O4. The addition of magnetite nanoparticles has been reported to improve the adsorption ability of the graphite waste. In this study, we have developed a new carbon dioxide (CO2) adsorbent based on graphite waste modified with magnetite nanoparticle Fe3O4. The Fe3O4 were prepared using an impregnation technique. The graphite/Fe3O4 composites were characterized by scanning electron microscopy with an energy-dispersive X-ray system (SEM-EDX) and Brunauer, Emmett, and Teller (BET). The CO2 adsorption performance was evaluated using an isothermal adsorption method at various temperatures (30, 35, and 45oC) and pressures (3, 5, 8, 15, and 20 bar). This resulted in graphite with different magnetite modification levels, namely non-modified graphite (GNM), a graphite/Fe3O4 20% (w/w) composite (G/Fe3O4 20%), and a graphite/Fe3O4 35% (w/w) (G/Fe3O4 35%), which indicated that the largest adsorption capacity is 10.305 mmol.g-1 at 30oC and 20 bar pressure for the G/Fe3O4 20% composite. This finding further revealed that modifying graphite waste with magnetite nanoparticles Fe3O4 has been proved to increase the capacity for adsorbing CO2 gas."

"ABSTRAKMelimpahnya limbah grafit dapat diolah menjadi bahan bernilai jual, salah satunya dengan menjadikannya sebagai adsorben. Rekayasa adsorben berbasis grafit dapat dilakukan dengan menambahkan nanopartikel magnetit berupa Fe3O4. Penambahan nanopartikel magnetit pada adsorben dilaporkan mampu mengadsorpsi gas lebih baik. Pada penelitian ini, dilakukan rekayasa limbah grafit yang dimodifikasi dengan menambahkan nanopartikel magnetit Fe3O4 menggunakan teknik impregnasi untuk diujicobakan dalam mengadsorpsi gas karbon dioksida CO2 sehingga diharapkan akan diperoleh alternatif adsorben yang mampu mengadsorpsi gas karbon dioksida CO2 dengan baik. Pada penelitian ini dilakukan pengujian adsorpsi gas CO2 menggunakan metode adsorpsi isotermal dengan variasi berupa suhu 300, 350, dan 450C serta tekanan 3,5,8,15, dan 20 Bar . Dari hasil uji coba menggunakan tiga jenis bahan yaitu grafit non modifikasi GNM , grafit/ Fe3O4 20 G/ Fe3O4 20 serta grafit/Fe3O4 35 G/ Fe3O4 35 melalui metode adsorpsi isotermal diperoleh kapasitas adsorpsi terbesar sebanyak 0,453 kg/kg pada suhu 300C dan tekanan 20 Bar menggunakan bahan grafit/Fe3O4 20 . Dengan demikian limbah grafit yang dimodifikasi dengan penambahan Fe3O4 mampu mengadsorpsi gas CO2 sama baiknya dengan adsorben lain.

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ABSTRACTThe abundance of graphite waste can be processed into valuable materials, one alternative is by making it as an adsorbent. Graphite based adsorbent modification can be accomplished by adding nanoparticle magnetic of Fe3O4 The addition of magnetite nanoparticles is reported can improve graphite rsquo s adsorption ability. In this research, we will modify the graphite waste by adding Fe3O4 magnetite nanoparticles using impregnation technique. The modified graphite is then tested using carbon dioxide gas CO2 to see how good its adsorption ability as a gas adsorbent. In this research, the CO2 adsorption testing will be carried out using isothermal adsorption method with temperature 300, 350, and 450C and pressure 3,5,8,15, and 20 Bar variations. The experimental result, by using three types of materials non modified graphite GNM , graphite Fe3O4 20 G Fe3O4 20 and graphite Fe3O4 35 G Fe3O4 35 it can be concluded that the largest adsorption capacity is 0,453 kg kg at 300C and 20 Bar pressure using material G Fe3O4 20 . Thus, the modified graphite waste with the addition of Fe3O4 is capable of adsorbing CO2 gas as well as other adsorbents."