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"Phase trnasformation temperature of shape memory alloy - Tini produced by arc - melting technique. The observation of phase trnasformation temperature of Tini alloys produced by arc - melting technique was carried out by alloying Ti - 53%w Ni. Tini alloys were tempered at 900oC and then followed by quenching at 20oC and 5oC and finally were aged at 400oC for 1,4 and 16 hours. The Ti-53%. Ni alloyed is applied to obtain as shape memory alloys base on Tini . The Tini sample was analyzed by optical microscope, X - ray diffraction and simultaneous symmetrical thermoanalyzer (STA) . The result show that the martensitic phase has a structure of BCT (bODY CENTER TETRAGONAL) formed at room temperarure. The phase transformation temperature from martensitic - austensitic phase was taken place at (162+5)oC"

"ABSTRAKPaduan Heusler Ni-Mn-Sn adalah salah satu material yang menjadi perhatianbanyak peneliti, karena memiliki potensi menghasilkan Magnetocaloric Effect(MCE) terutama dalam penerapan berbagai aplikasi bidang magnetik. Padapenelitian ini telah dilakukan sintesis polikristalin Ni43Mn41Co5Sn11 menggunakan teknik vakum peleburan busur panas atau vacuum arc melting (VAM) pada temperatur tinggi dalam suasana kaya gas argon. Optimalisasi sifat magnetik paduan NMCS dilakukan pada temperatur 1173 K dengan variasi waktu anil selama 0, 6, 12, dan 24 jam hingga didapatkan fasa kristal yang homogen. Pola difraksi sinar-X pada sampel hasil anil terdiri dari fasa martensit dan austenit, dengan struktur kristal FCC pada temperatur ruang. Fasa dendrit material pasca peleburan telah bertransformasi menjadi fasa yang seragam seiring dengan variasi waktu anil yang diberikan untuk mencapai homogenisasi. Hasil identifikasi struktur kristal material pasca anil 6 dan 12 jam menyerupai tipe order Cu2MnAl, sedangkan untuk material pasca anil 24 jam menyerupai tipe order CsCl. Adapun pembentukan fasa NiMnCoSn pada sampel melalui pembentukan fasa antara yakni Ni2MnSn. Apabila dilihat dari nilai temperatur curie material NMCS tidak mengalami perubahan secara signifikan seiring dengan variasi waktu anil yaitu sekitar 348~351 K, namun pada efek perlakuan anil selama 12 jam menunjukan nilai magnetisasi terbesar sekitar 57.96 emu/g dengan koersivitas 45.60 Oe. Hasil penelitian ini menyimpulkan bahwa sintesa material magnetokalorik paduan heusler Ni43Mn41Co5Sn11 melalui teknik peleburan vakum yang dilanjutkandengan perlakuan anil selama 12 jam dapat menjadi salah satu cara dalampembuatan material MCE berbasis paduan heusler

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ABSTRACTNi?Mn?Sn Heusler alloys have been attracting alot of scientists by virtue of their magnetocaloric effect and application potential for magnetic refrigeration at room temperature. In this work, policrystalline Ni43Mn41Co5Sn11 alloy has been synthesized by vacuum arc-melting of pure elements under protective Aratmosphere. The optimization of magnetic properties of the NMCS alloy wasobtained during the annealing times at 1173 K by various annealing times 0, 6, 12, and 24 hours. X-ray diffraction patterns showed that the annealed samples were in the mixed martensite-austenite phase, revealed that the alloy has a FCC crystal structure as the main phase at room temperature. A result confirmed that the dendritic structure transformed into the uniform crystal structure of varying annealing time in order to attain homogeneous alloy. The crystal structure identification of the material after the annealing 6 and 12 hours showed Cu2MnAl order type, and the annealed material for 24 hours showed CsCl order type. The NiMnCoSn phase formation in a sample through a phase formation in the middle the Ni2MnSn. The curie temperature of the NMCS material was not change significantly during variation of annealing time around 348~351 K, but the effect of annealing for 12 hour showed the greatest magnetization value at 57.96 emu/g and also the coercivity at 45.60 Oe. The results of this study concluded that synthesis of heusler alloy Ni43Mn41Co5Sn11 through vacuum melting techniques, followed by annealing for 12 hours has proven to be alternative route for material MCE-based heusler alloys fabrication."