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"Materials science and engineering of carbon, fundamentals provides a comprehensive introduction to carbon, the fourth most abundant element in the universe. The contents are organized into two main parts. Following a brief introduction on the history of carbon materials, Part 1 focuses on the fundamental science on the preparation and characterization of various carbon materials, and Part 2 concentrates on their engineering and applications, including hot areas like energy storage and environmental remediation. The book also includes up-to-date advanced information on such newer carbon-based materials as carbon nanotubes and nanofibers, fullerenes and graphenes."

"Materials science and engineering of carbon : fundamentals provides a comprehensive introduction to carbon, the fourth most abundant element in the universe. The contents are organized into two main parts. Following a brief introduction on the history of carbon materials, Part 1 focuses on the fundamental science on the preparation and characterization of various carbon materials, and Part 2 concentrates on their engineering and applications, including hot areas like energy storage and environmental remediation. The book also includes up-to-date advanced information on such newer carbon-based materials as carbon nanotubes and nanofibers, fullerenes and graphenes."

"Materials science and engineering of carbon: fundamentals provides a comprehensive introduction to carbon, the fourth most abundant element in the universe. The contents are organized into two main parts. Following a brief introduction on the history of carbon materials, Part 1 focuses on the fundamental science on the preparation and characterization of various carbon materials, and Part 2 concentrates on their engineering and applications, including hot areas like energy storage and environmental remediation."

"Modifikasi elektroda glassy carbon (GC) sebagai sensor kimia parasetamol dikembangkan secara molecular imprinted polymer (MIP). Pembentukan lapisan polimer polifenol atau polianilin pada permukaan elektroda GC di sekeliling parasetamol sebagai molekul cetakan dilakukan dengan teknik elektropolimerisasi secara voltametri siklik. Hasil optimasi pembuatan elektroda GC MIP fenol pada perbandingan konsentrasi fenol dan parasetamol 1x10-4 M : 1x10-2 M, diperoleh nilai sensitivitas 0,0183 µA/ppm dan batas deteksi 3,9786 ppm. Modifikasi elektroda GC MIP fenol pada pengukuran persen kadar parasetamol yang kelinieran diperoleh pada rentang konsentrasi 10 ppm sampai 700 ppm. Aplikasi untuk obat komersial Parasetamol tablet didapatkan kadar 98,38 % dan Bodrex® tablet adalah 95,21%. Hasil optimasi elektroda GC MIP anilin pada perbandinagn konsentrasi anilin dan parasetamol 1x10-1 M : 1x10-2 M, diperoleh nilai sensitivitas 0.0243 µA/ppm dan batas deteksi 2,2010 ppm, untuk elektroda GC MIP anilin kelinieran diperoleh pada rentang konsentrasi 10 ppm sampai 1200 ppm. Aplikasi pada sampel obat komersial parasetamol 100,90 % dan Bodrex® diperoleh 97,18%. Berdasarkan penelitian dan aplikasi pada sampel obat, analisis dengan menggunakan elektroda GC MIP dibandingkan dengan metode KCKT kedua metode tersebut masuk dalam rentang persyaratan yang terdapat pada Farmakope Indonesia.

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The modification of glassy carbon (GC) electrodes as paracetamol chemical sensors has been develoved by using molecular imprinted polymer (MIP) based on polyphenol and polyaniline. The formation of polyphenols or polyaniline polymer layer on the surface of GC electrodes as the molecular molding around the paracetamol molecule is performed electrochemically using cyclic voltammetry technique. For polyphenol based MIP fabrication, phenol to paracetamol concentration ratio with the value of 1x10-4 M : 1x10-2 M gives the optimum results giving the sensitivity value 0.0183 A/ppm and LOD 3.9786 ppm. The modified electrode also shows a linearity in the paracetamol concentration range between 10 to 700 ppm. In addition the paracetamol detected using the modified electrodes reveals 98.38% and 95.61% similarity to that of shown on the label of Paracetamol and Bodrex® respectively. Meanwhile, for polyaniline-based MIP fabrication the optimum aniline to paracetamol concentration ratio is 1x10-1 M : 1x10-2 M which gives the sensitivity value 0.0243 A/ppm, LOD 2.2010 ppm and range of linearity 10 to 1200 ppm. In respect of commercial medicine application, the detection using polyaniline-based modified electrode shows 100.90% and 97.18% similiarites to that of shown on the label of Paracetamol and Bodrex® respectively. The detection of paracetamol using both MIP modefied electrodes is also comparable to the detection using conventional method such as HPLC."

"Pelat bipolar merupakan komponen utama dalam Polymer Electrolyte Membrane Fuel Cell (PEMFC). Pada penelitian ini pelat bipolar dibuat dari grafit komposit yang terdiri dari matriks grafit Electric Arc Furnace (EAF), carbon black sebagai pengisi, dan resin epoksi sebagai pengikat. Semua bahan dicampur dengan menggunakan high speed mixer dengan variabel komposisi dari carbon black ISAF N220 0%, 2.5%, 5%, 7.5%, dan 10%.Metode compression moulding dilakukan dalam pembuatan pelat bipolar dengan menggunakan tekanan 55 MPa selama 4 jam pada temperatur 100°C. Material dikarakterisasi melalui pengujian tarik, pengujian fleksural, pengujian densitas, pengujian porositas, pengujian konduktivitas listrik, dan pengujian Field Electron Scanning Electron Microscope (FESEM).Hasil penelitian menunjukkan bahwa pada komposisi carbon black 10% menghasilkan pelat bipolar dengan karakteristik optimum dengan nilai konduktivitas tertinggi sebesar 7,07 S/cm. Kekuatan fleksural sebesar 51,34 MPa. Namun demikian, densitas terendah sebesar 1,96 gr/cm3 diperoleh dengan melakukan pencampuran carbon black 0% , dan porositas terkecil 0,49% diperoleh pada komposisi carbon black 10%. Pengamatan visual menunjukkan bahwa seluruh pelat bipolar mempunyai penampakan yang baik, tidak retak, dan permukaan yang rata.

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Bipolar plate is a major component in Polymer Electrolyte Membrane Fuel Cell (PEMFC). In this study bipolar plates made of graphite composite consisting of a matrix of graphite Electric Arc Furnace (EAF), carbon black as filler, and epoxy resin as a binder. All the ingredients are mixed using a high speed mixer with variable composition of carbon black ISAF N220 0%, 2.5%, 5%, 7.5%, and 10%.

Methode of compression molding is done in the manufacture of bipolar plates using a pressure of 55 MPa for 4 hours at a temperature of 100°C.

The results showed that the composition of 10% carbon black produce bipolar plates with optimum characteristics with the highest conductivity value of 7.07 S / cm. Fleksural strength of 51.34 MPa. However, the lowest density of 1.96 gr/cm3 obtained by mixing carbon black 0%, and the smallest porosity of 0,49% is obtained on the composition of 10% carbon black. Visual observations showed that all bipolar plates have a good appearance, no cracks, and a flat surface."

"Composite materials, offers integrated and completely up-to-date coverage of composite materials. The book focuses on the triad of processing, structure, and properties, while providing a well-balanced treatment of the materials science and mechanics of composites. In this edition, revised and updated throughout, increasing use of composites in industry (especially aerospace and energy) and new developments in the field are highlighted. There is a new chapter on non-conventional composites, which covers polymer, metal and ceramic matrix nanocomposites, self-healing composites, self-reinforced composites, biocomposites and laminates made of metals and polymer matrix composites. Examples of practical applications in various fields are given throughout the book. "

"Pelat bipolar merupakan komponen penting di dalam Polymer Electrolyte Membrane Fuel Cell (PEMFC) yang berfungsi untuk mengumpulkan dan memindahkan elektron dari anoda ke katoda. Pelat bipolar berbasis komposit terdiri dari grafit sintetis (MERCK) dan carbon black sebagai filler serta resin epoksi dan hardener sebagai binder. Carbon black dibuat dari pembakaran serabut kelapa pada suhu 500°C dan 900°C dalam kondisi inert. Pembahasan utama pada penelitian ini adalah menganalisis pengaruh variasi komposisi ukuran partikel carbon black sebagai variabel pertama dan lama pencampuran grafit dan carbon black dalam media air sebagai variabel kedua, terhadap distribusi sifatsifat pelat bipolar PEMFC berbasis komposit epoksi/grafit. Komposisi ukuran partikel carbon black hasil milling dengan rotary ball mill selama 2 hari berbanding 4 hari pada penelitian ini, yaitu 5:95, 10:90, 15:85 dan 20:80. Lama pencampuran antara grafit dan carbon black divariasikan dari 1 jam, 2 jam, 3 jam dan 4 jam dengan alat hand mixer di dalam media air. Pelat bipolar dicetak dengan metode compression molding dengan tekanan 55 MPa selama 4 jam pada suhu 100oC. Karakterisasi pelat bipolar meliputi pengujian konduktivitas listrik, pengujian fleksural, pengujian densitas, pengujian porositas, analisis gugus fungsional dengan FTIR dan pengamatan permukaan patahan fleksural menggunakan FE-SEM. Hasil penelitian menunjukkan bahwa komposisi optimal ukuran partikel carbon black hasil milling 2 hari dan 4 hari dengan perbandingan 15:85 pada lama pencampuran 3 jam dalam media air menghasilkan pelat bipolar dengan karakteristik nilai konduktivitas tertinggi sebesar 1.06 S/cm, kekuatan fleksural 48.38 MPa, densitas 2.50 gr/cm3 dan porositas 0.70%.

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Bipolar plate is one of main components in Polymer Electrolyte Membrane Fuel Cell (PEMFC) that collects and transfers electron from anode to cathode. Bipolar plate composites consist of syntetic graphite (MERCK) and carbon black (CB) as filler material. Epoxy resin and hardener was used as binder material of the composite. Carbon black was prepared from combustion of palm fiber in 500 and 900°C through inert atmosphere. The main discussion in this research is to investigate the influence of variations in composition of carbon black particle size and mixing time of graphite and carbon black to the distribution of properties of PEMFC bipolar plates based on graphite/epoxy composite. Particle size composition ratio of milled carbon black in 2 days and 4 days are 5:95, 10:90, 15:85 and 20:80. Variation in mixing time of graphite and carbon black are 1 hour, 2 hours, 3 hours and 4 hours with water as mixing media. Characterization of bipolar plate material includes electrical conductivity test. flexural test, density and porosity measurement, functional groups analysis using FTIR and fracture surface examination using FE-SEM. The optimum composition was obtained in ratio of 2 days milled-CB : 4 days milled-CB in range of 15:85 and 3 hours mixing time using water. The optimum electrical conductivity, flexural strength, density and porosity were respectively: 1.06 S/cm, 48.38 MPa, 2.50 gr/cm3 and 0.70%."

"Dewasa ini penggunaan material komposit serat karbon mulai banyak digunakan dalam berbagai sektor industri karena memiliki sifat-sifat yang mampu memenuhi tuntutan teknologi, seperti ringan, tahan fatik, dan tahan terhadap temperatur tinggi. Penelitian terhadap perfoma komposit serat karbon baik termal dan mekanik masih jarang dilakukan. Oleh karena itu dilakukanlah pengujian untuk mengetahui hal tersebut. Komposit serat karbon yang digunakan memiliki variasi densitas berbeda yaitu 200 dan 240 gr/m2Metode yang digunakan dalam penelitian ini berbasis pada kalorimeter kerucut. Pembakaran dilakukan pada nilai fluks kalor maksimum 23,61 kW/m2 dan minimum 14,15 kW/m2. Pada penelitian ini juga dilakukan pengujian tarik dan SEM untuk mengetahui sifat mekanik dari komposit serat karbon. Hasil dari penelitian ini menunjukkan semakin tinggi fluks kalor, maka laju produksi kalor dari pembakaran komposit serat karbon juga meningkat dimana laju produksi maksimum yang dicapai bernilai 160-170 kW/m2. Sementara itu dari pengujian mekanik didapatkan bahwa material komposit serat karbon memiliki sifat diantara ulet dan getas.

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In this present days, the use of carbon fiber composite material used widely in various industrial sectors. This happens because carbon fiber composite have good properties that can fulfill the demands of technology requirements, such as lightweight, fatigue resistant, and withstand to high temperatures. Studies on carbon fiber composites performance, especially regarding its thermal and mechanical performance, are still not observed widely. Carbon fiber composites used in this study has density of 200 and 240 gr/m2.

The method used in this study based on cone calorimeter. Combustion was performed onthe maximum heat flux of 23.61 kW/m2 and a minimum heat flux of 14.15 kW/m2. This study also used the tensile test and SEM analysis to determine the mechanical properties of carbon fiber composites.

The results of this study showed that at the higher heat flux, the heat release rate (HRR) carbon fiber composites was increased withthe maximum valueof 160-170 kW/m2. Meanwhile, analysis of mechanical properties showed that the carbon fiber composite material has a characteristic between ductile and brittle."

"Kondisi lingkungan dapat memberikan efek yang sangat besar dalam bentuk kegagalan komposit karbon/epoksi. Kondisi lingkungan menjadi perhatian dalam dunia penerbangan karena dapat mempengaruhi kekuatan mekanik dan sifat termal dari material yang dijadikan bahan penyusun struktur pesawat. Penelitian ini dilakukan untuk mengetahui pengaruh kondisi lingkungan, khususnya kemampuan penyerapan kadar air, kekuatan mekanik, sifat termal, dan jenis kerusakan dari komposit karbon/epoksi unidirectional. Komposit ini dibuat dengan metode dry hand lay-up. Untuk mengetahui hal tersebut, komposit karbon diberikan kondisi lingkungan yang berbeda, yaitu keadaan tanpa perendaman, direndam dalam air panas, dan air laut dalam waktu tertentu. Dari hasil pengamatan penyerapan kadar air dari, didapatkan kandungan kadar air maksimum yang terserap ke dalam komposit karbon/epoksi dalam lingkungan air panas 0,89 selama 1100 jam dan air laut 0,57 selama 1200 jam perendaman. Uji mekanik short-beam shear menunjukkan persentase penurunan nilai kekuatan antarlamina dari hasil uji mekanik pada keadaan air panas dan air laut berturut-turut sebesar 9,66 dan 0,92 dibandingkan dengan bahan tanpa perendaman. Suhu transisi gelas relatif sama dari tiap kondisi lingkungan. Hasil pengamatan mikroskop optik dan Scanning Electron Microscope tidak memperlihatkan perbedaan yang berarti dari ketiga komposit. Jadi material komposit karbon/epoksi unidirectional tidak mengalami perubahan berarti pada sifat termal dan kerusakan permukaan akibat pengaruh air panas dan air laut.

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Environmental conditions can result a profound effect in a forms of carbon epoxy composite failures. Environmental conditions are one of the main considerations in the aerospace industry as they can affect the mechanical strength and thermal properties of the materials that be used as aircraft structures. This study was aimed to determine the effect of environmental conditions, especially the moisture absorption, mechanical strength, thermal properties, and types of damage of unidirectional carbon epoxy composites. The composites were fabricated by a dry hand lay up process. The composites were conditioned in different environment which were normal condition or without immersion, soaked in both hot water, and seawater within a certain time. The maximum moisture content that was absorbed in the composites was 0.89 for 1100 hours in hot water and was 0.57 in seawater for 1200 hours of immersion. Furthermore, short beam shear test results showed that the interlaminate strength values reduced 9.66 and 0.92 in hot water and sea water conditions respectively compared to composites in normal condition. The glass transition temperature of hot water and sea water conditioned materials were relatively similar compared to materials in normal condition. According to optical microscope and Scanning Electron Microscope observations, there was no visible difference on the surface of three materials. Thus, the thermal property and the appearance of the unidirectional carbon epoxy composites did not change in hot water and sea water."